2-(2-naphthyl)thiophene

Base Information

• Chemical Name: 2-(2-naphthyl)thiophene
• CAS No.: 16939-09-6
• Molecular Formula: C14H10S
• Molecular Weight: 210.29400
• Mol file: 16939-09-6.mol

Synonyms:2-(naphth-2-yl)thiophene;2-(2-naphthyl)thiophene;2-(naphthalen-2-yl)thiophene;2-(2-thienyl)naphthalene;2-(thien-2-yl)naphthalene;2-Naphthalen-2-yl-thiophene;2-naphthalen-2-ylthiophene;

Chemical Property of 2-(2-naphthyl)thiophene

Chemical Property:

• Melting Point: 102 °C
• PSA: 28.24000
• LogP: 4.56830

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-naphthyl)thiophene

There total 29 articles about 2-(2-naphthyl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

thiophene boronic acid (6165-68-0) + 2-bromonaphthalene (580-13-2) → 2-naphthalen-2-yl-thiophene (16939-09-6)

Guidance literature:

With potassium carbonate; [PS-PEG-adppp-Pd(η³-C3H5)]Cl; In water; at 50 ℃; for 12h;

DOI:10.1021/ol0264298

Reference yield: 98.0%

2-naphthalenecarbonitrile (613-46-7) + thiophen-2-ylmanganese(II) chloride (145091-61-8) → 2-naphthalen-2-yl-thiophene (16939-09-6)

Guidance literature:

With dichlorobis(trimethylphosphine)nickel; In tetrahydrofuran; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1002/adsc.201200369

Reference yield: 98.0%

2-iodonaphthalene (612-55-5) + thiophen-2-ylzinc iodide (45438-82-2) → 2-naphthalen-2-yl-thiophene (16939-09-6)

Guidance literature:

With lithium chloride; In tetrahydrofuran; toluene; at 110 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201308200

upstream raw materials:

thiophene

2-bromonaphthalene

2-naphthyl triflate

tributyl(thien-2-yl)stannane