(1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate

Base Information

• Chemical Name: (1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate
• CAS No.: 131244-12-7
• Molecular Formula: C₃₂H₃₉O₄PS
• Molecular Weight: 550.699

Synonyms:

Chemical Property of (1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate

There total 1 articles about (1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-t-butyl thiopropenoate (19737-45-2) + 2-methyl-2-cyclopenten-1-one (1120-73-6) + trans-crotyldiphenylphosphine oxide (17668-60-9) → (1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate (131244-12-7) + S,S'-di-t-butyl 1<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-3a-hydroxy-7a-methyl-octahydro-1H-indene-4,6-dicarbothioate (131228-05-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1071/CH9901375

upstream raw materials:

S-t-butyl thiopropenoate

2-methyl-2-cyclopenten-1-one

trans-crotyldiphenylphosphine oxide

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