S-t-butyl thiopropenoate

Base Information

• Chemical Name: S-t-butyl thiopropenoate
• CAS No.: 19737-45-2
• Molecular Formula: C₇H₁₂OS
• Molecular Weight: 144.238

Synonyms:S-t-butyl thiopropenoate

Chemical Property of S-t-butyl thiopropenoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of S-t-butyl thiopropenoate

There total 2 articles about S-t-butyl thiopropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-tert-Butylsulfanylcarbonyl-ethyl)-trimethyl-ammonium → S-t-butyl thiopropenoate (19737-45-2) + trimethylamine (75-50-3)

Guidance literature:

In water; at 30 ℃; Equilibrium constant;

DOI:10.1021/ja01032a020

Reference yield:

2-methylpropan-2-thiol (75-66-1) + acetylene (74-86-2,25067-58-7) → S-t-butyl thiopropenoate (19737-45-2) + butanone (78-93-3)

Guidance literature:

With carbon monoxide; tetracarbonyl nickel; acrylic acid;

Reference yield: 48.0%

1-phenyl-1-trimethylsiloxypropene (37471-46-8) + S-t-butyl thiopropenoate (19737-45-2) → S-t-butyl 4-methyl-5-oxo-5-phenyl-pentanethioate (116409-49-5)

Guidance literature:

With antimonypentachloride; tin(ll) chloride; In dichloromethane; at -78 ℃; for 4h;

DOI:10.1016/0022-328X(90)85213-I

upstream raw materials:

2-methylpropan-2-thiol

acetylene

Downstream raw materials:

S-t-butyl 4-methyl-5-oxo-5-phenyl-pentanethioate

(1'RS,2'E,3SR,4aSR,5SR,7aRS,8RS)-5-<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-4a-methyl-2-oxo-hexahydro-3,7a-ethano-2H-cyclopentapyran-8-carbothioate

S,S'-di-t-butyl 1<3'-(diphenylphosphinoyl)-1'-methylprop-2'-enyl>-3a-hydroxy-7a-methyl-octahydro-1H-indene-4,6-dicarbothioate

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