2-bromoethyl phenylcarbamate

Base Information

• Chemical Name: 2-bromoethyl phenylcarbamate
• CAS No.: 32353-12-1
• Molecular Formula: C₉H₁₀BrNO₂
• Molecular Weight: 244.088
• Mol file: 32353-12-1.mol

Synonyms:Ethanol,2-bromo-, carbanilate (6CI,7CI,8CI); N-(2-Bromoethoxycarbonyl)aniline; NSC220027

Chemical Property of 2-bromoethyl phenylcarbamate

Chemical Property:

• Vapor Pressure: 0.00703mmHg at 25°C
• Boiling Point: 270°C at 760 mmHg
• Flash Point: 117.1°C
• Density: 1.539g/cm³

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromoethyl phenylcarbamate

There total 3 articles about 2-bromoethyl phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl isocyanate (103-71-9) + 2-bromoethanol (540-51-2) → 2-bromoethyl phenylcarbamate (32353-12-1)

Guidance literature:

DOI:10.1021/i560108a014 DOI:10.1039/jr9420000737

Reference yield:

aniline (62-53-3) + 2-bromoethyl chloroformate (4801-27-8) → 2-bromoethyl phenylcarbamate (32353-12-1)

Guidance literature:

With pyridine; In dichloromethane;

Reference yield:

→ 2-bromoethyl phenylcarbamate (32353-12-1)

Guidance literature:

BrCH2CH2OH, PhNCO;

DOI:10.1021/jo00968a021

upstream raw materials:

phenyl isocyanate

2-bromoethanol

aniline

2-bromoethyl chloroformate

Downstream raw materials:

N-<2-(Methyldiphenylphosphonio)ethoxycarbonyl>anilin-bromid

Br^(1-)*C₁₉H₁₉N₂O₂⁽¹⁺⁾

Br^(1-)*C₂₇H₂₅N₄O₂S⁽¹⁺⁾