[2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester

Base Information

• Chemical Name: [2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester
• CAS No.: 120969-74-6
• Molecular Formula: C₃₈H₅₆N₈O₄P₂S₂
• Molecular Weight: 814.993

Synonyms:

Chemical Property of [2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester

Chemical Property:

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Technology Process of [2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester

There total 1 articles about [2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylentetramine (112-24-3) + 3-Dimethylaminophenol (99-07-0) → [2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester (120969-74-6)

Guidance literature:

Multistep reaction; (i) PSCl₃, Et₃N, (ii) /BRN= 605448/, KOH;

Reference yield:

[2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester (120969-74-6) + chlorothiophosphoric acid O,O'-bis-(4-dimethylamino-phenyl ester) (132886-53-4) → C70H94N12O8P4S4 (111474-81-8)

Guidance literature:

With N,N'-dimethylbenzylamine;

Reference yield:

[2-(2-{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethylamino}-ethylamino)-ethyl]-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester (120969-74-6) + 4-bromobenzenesulfonyl chloride (98-58-8) → {2-[{2-[{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethyl}-(4-bromo-benzenesulfonyl)-amino]-ethyl}-(4-bromo-benzenesulfonyl)-amino]-ethyl}-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester (109016-25-3)

Guidance literature:

With N,N'-dimethylbenzylamine;

upstream raw materials:

triethylentetramine

3-Dimethylaminophenol

Downstream raw materials:

C₇₀H₉₄N₁₂O₈P₄S₄

{2-[{2-[{2-[Bis-(3-dimethylamino-phenoxy)-thiophosphorylamino]-ethyl}-(4-bromo-benzenesulfonyl)-amino]-ethyl}-(4-bromo-benzenesulfonyl)-amino]-ethyl}-thiophosphoramidic acid O,O'-bis-(3-dimethylamino-phenyl) ester

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