N-(2-Phenyl-ethenyl)-piperidin-2-one

Base Information

Chemical Name:N-(2-Phenyl-ethenyl)-piperidin-2-one
CAS No.:17179-93-0
Molecular Formula:C13H15NO
Molecular Weight:201.268
Hs Code.:
DSSTox Substance ID:DTXSID701277897

Synonyms:N-(2-Phenyl-ethenyl)-piperidin-2-one;AYQKOMRRXJYQHX-PKNBQFBNSA-N;DTXSID701277897;1-[(1E)-2-Phenylethenyl]-2-piperidinone;1-[(E)-2-Phenylethenyl]-2-piperidinone #;17179-93-0

Suppliers and Price of N-(2-Phenyl-ethenyl)-piperidin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-Phenyl-ethenyl)-piperidin-2-one

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:201.115364102
Heavy Atom Count:15
Complexity:241

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(C(=O)C1)C=CC2=CC=CC=C2
Isomeric SMILES:C1CCN(C(=O)C1)/C=C/C2=CC=CC=C2

Technology Process of N-(2-Phenyl-ethenyl)-piperidin-2-one

There total 4 articles about N-(2-Phenyl-ethenyl)-piperidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 675-20-7
piperidin-2-one

: 122-78-1
phenylacetaldehyde

: 17179-93-0
(E)-N-(2-phenylethenyl)-2-piperidinone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;

Reference yield: 32.0%

: 675-20-7
piperidin-2-one

: 536-74-3
phenylacetylene

: 24904-52-7
(Z)-N-(2-phenylethenyl)-2-piperidinone

: 17179-93-0
(E)-N-(2-phenylethenyl)-2-piperidinone

Guidance literature:: With hexa[tri(dimethylamino)phosphazene]cyclotriphosphazene; In dimethyl sulfoxide; at 120 ℃; for 24h; Overall yield = 58 %; stereoselective reaction; Inert atmosphere; Glovebox;
DOI:10.1016/j.tet.2019.04.075

Reference yield:

: 675-20-7
piperidin-2-one

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 17179-93-0
(E)-N-(2-phenylethenyl)-2-piperidinone

Guidance literature:: With copper(l) iodide; potassium hydride; Yield given. Multistep reaction; 2) HMPA, 130 deg C, 5h;
DOI:10.1246/cl.1991.1443