[RuCl(CO)(PPh₃)2(2-(benzylimino methyl)-4-methoxyphenol)]

Base Information

• Chemical Name: [RuCl(CO)(PPh₃)2(2-(benzylimino methyl)-4-methoxyphenol)]
• CAS No.: 1219710-77-6
• Molecular Formula: C₅₂H₄₄ClNO₃P₂Ru
• Molecular Weight: 929.397
• Mol file: 1219710-77-6.mol

Synonyms:

Chemical Property of [RuCl(CO)(PPh₃)2(2-(benzylimino methyl)-4-methoxyphenol)]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [RuCl(CO)(PPh₃)2(2-(benzylimino methyl)-4-methoxyphenol)]

There total 1 articles about [RuCl(CO)(PPh₃)2(2-(benzylimino methyl)-4-methoxyphenol)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris(triphenylphosphine)ruthenium(II) chloride (15529-49-4,41756-81-4) + 2-(benzylimino methyl)-4-methoxyphenol (258354-71-1) → [RuCl(CO)(PPh3)2(2-(benzylimino methyl)-4-methoxyphenol)] (1219710-77-6)

Guidance literature:

In methanol; solid Ru compd. added to MeOH soln. of ligand and Et3N (0.2:0.4:0.43 molar ratio), mixt. refluxed for 5 h; pptd. on cooling, filtered off, washed (n-hexane), dried in air, dissolved (CH2Cl2), chromd. (Al2O3, CH2Cl2, CH2Cl2/5% acetone), recrystd. (CH2Cl2/n-hexane), elem. anal.;

DOI:10.1016/j.jorganchem.2009.11.020

upstream raw materials:

tris(triphenylphosphine)ruthenium(II) chloride

2-(benzylimino methyl)-4-methoxyphenol