1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-

Base Information

Chemical Name:1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-
CAS No.:171824-52-5
Molecular Formula:C21H13N3O6
Molecular Weight:403.351
Hs Code.:
DSSTox Substance ID:DTXSID20455614
Wikidata:Q82277699
Mol file:171824-52-5.mol

Synonyms:1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-;171824-52-5;SCHEMBL6995634;DTXSID20455614

Suppliers and Price of 1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:403.08043514
Heavy Atom Count:30
Complexity:671

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=O)C2=C(C=CC(=C2C1=O)C3=CC=CC=C3[N+](=O)[O-])C4=CC=CC=C4[N+](=O)[O-]

Technology Process of 1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)-

There total 4 articles about 1H-Isoindole-1,3(2H)-dione, 2-methyl-4,7-bis(2-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2-Methyl-4,7-bis-(2-nitro-phenyl)-3a,4,7,7a-tetrahydro-isoindole-1,3-dione

: 171824-52-5
2-Methyl-4,7-bis-(2-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In various solvent(s); at 165 ℃; for 18h;
DOI:10.1016/0040-4039(95)01811-U

Reference yield:

: 1466-88-2,66894-06-2
2-nitrocinnamic aldehyde

: 171824-52-5
2-Methyl-4,7-bis-(2-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LiOMe; 2.) I₂ / 1.) MeOH; 2.) MePh, reflux

2: 96 percent / 12 h / 120 °C

3: 89 percent / DDQ / various solvent(s) / 18 h / 165 °C

With lithium methanolate; iodine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In various solvent(s);
DOI:10.1016/0040-4039(95)01811-U

Reference yield:

: 87259-89-0
(E,E)-1,4-bis(2-nitrophenyl)buta-1,3-diene

: 171824-52-5
2-Methyl-4,7-bis-(2-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 12 h / 120 °C

2: 89 percent / DDQ / various solvent(s) / 18 h / 165 °C

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In various solvent(s);
DOI:10.1016/0040-4039(95)01811-U