(NE)-N-benzylidene-1-phenylmethanesulfonamide

Base Information

Chemical Name:(NE)-N-benzylidene-1-phenylmethanesulfonamide
CAS No.:58908-07-9
Molecular Formula:C14H13 N O2 S
Molecular Weight:259.329
Hs Code.:
NSC Number:280067
DSSTox Substance ID:DTXSID20429693

Synonyms:NSC280067;58908-07-9;DTXSID20429693;NSC-280067

Suppliers and Price of (NE)-N-benzylidene-1-phenylmethanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (NE)-N-benzylidene-1-phenylmethanesulfonamide

Chemical Property:

Vapor Pressure:3.18E-07mmHg at 25°C
Boiling Point:430.7°C at 760 mmHg
Flash Point:214.3°C
Density:1.14g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:259.06669983
Heavy Atom Count:18
Complexity:358

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CS(=O)(=O)N=CC2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)CS(=O)(=O)/N=C/C2=CC=CC=C2

Technology Process of (NE)-N-benzylidene-1-phenylmethanesulfonamide

There total 6 articles about (NE)-N-benzylidene-1-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 774-48-1
(diethoxymethyl)benzene

: 4563-33-1
phenyl-methanesulfonic acid amide

: 58908-07-9
N-Benzyliden-toluol-ω-sulfonsaeureamid

Guidance literature:: at 150 - 180 ℃; for 0.5h;
DOI:10.1021/ja00526a040

Reference yield: 44.0%

: 4563-33-1
phenyl-methanesulfonic acid amide

: 100-52-7
benzaldehyde

: 58908-07-9
N-Benzyliden-toluol-ω-sulfonsaeureamid

Guidance literature:: With trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; In 1,2-dichloro-ethane; at 35 ℃; for 3h;
DOI:10.1002/jhet.5570230620

Reference yield:

: 57267-76-2
sodium α-toluenesulfonate

: 58908-07-9
N-Benzyliden-toluol-ω-sulfonsaeureamid

Guidance literature:: Multi-step reaction with 4 steps

1: Phosphorus pentachloride

2: CHCl₃; benzene

3: 9 percent / Trioxane, CH₃SO₃H, Acetic anhydride / 1,2-dichloro-ethane / 4 h / 35 °C

4: 44 percent / Trifluoromethanesulphonic acid, Trifluoromethanesulphonic anhydride / 1,2-dichloro-ethane / 3 h / 35 °C

With methanesulfonic acid; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; Trioxane; phosphorus pentachloride; acetic anhydride; In chloroform; 1,2-dichloro-ethane; benzene;
DOI:10.1002/jhet.5570230620