Carbamic acid, [(1S)-1-[[[(1S)-1-(hydroxymethyl)-2-phenylethyl]amino]carbonyl]-3-methyl butyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-[[[(1S)-1-(hydroxymethyl)-2-phenylethyl]amino]carbonyl]-3-methyl butyl]-, 1,1-dimethylethyl ester
CAS No.:171978-60-2
Molecular Formula:C20H32N2O4
Molecular Weight:364.485
Hs Code.:
Mol file:171978-60-2.mol

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Chemical Property of Carbamic acid, [(1S)-1-[[[(1S)-1-(hydroxymethyl)-2-phenylethyl]amino]carbonyl]-3-methyl butyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [(1S)-1-[[[(1S)-1-(hydroxymethyl)-2-phenylethyl]amino]carbonyl]-3-methyl butyl]-, 1,1-dimethylethyl ester

There total 9 articles about Carbamic acid, [(1S)-1-[[[(1S)-1-(hydroxymethyl)-2-phenylethyl]amino]carbonyl]-3-methyl butyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3182-95-4
L-Phenylalaninol

: 200937-21-9
N-tert-butoxycarbonyl-L-leucine monohydrate

: 171978-60-2
tert-butyl ((S)-1-(((S)-1-hydroxy-3-phenylpropan-2-yl)-amino)-4-methyl-1-oxopentan-2-yl)carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.bmcl.2018.12.032

Reference yield: 84.0%

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 3182-95-4
L-Phenylalaninol

: 171978-60-2
tert-butyl ((S)-1-(((S)-1-hydroxy-3-phenylpropan-2-yl)-amino)-4-methyl-1-oxopentan-2-yl)carbamate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.joc.8b03206