9-Anthracenesulfonic acid sodium salt

Base Information

Chemical Name:9-Anthracenesulfonic acid sodium salt
CAS No.:17213-01-3
Molecular Formula:C14H10O3S.Na
Molecular Weight:280.279
Hs Code.:2904100000
Mol file:17213-01-3.mol

Synonyms:Anthracen-9-natriumsulfonat;Anthracen-9-sulfonsaeure, Natriumsalz;anthracene-9-sulfonic acid, sodium salt;Na-Salz der Anthracen-sulfonsaeure-(9);Sodium 9-anthracenesulfonate;

Suppliers and Price of 9-Anthracenesulfonic acid sodium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 9-Anthracenesulfonic acid sodium salt

Chemical Property:

PSA：65.58000
LogP:3.97790

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9-Anthracenesulfonic acid sodium salt

There total 1 articles about 9-Anthracenesulfonic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 602-60-8
9-nitroanthracene

: 7757-83-7
sodium sulfite

: 17213-01-3
sodium anthracene-9-sulfonate

: (9,9'-bianthracene)-10-sulphonic acid sodium salt

Guidance literature:: In not given; heating;

Reference yield:

: 17213-01-3
sodium anthracene-9-sulfonate

: 120-12-7
anthracene

: 84-65-1
9,10-phenanthrenequinone

Guidance literature:: With sodium hydroxide; for 3h; Mechanism; other sodium arenesulfonates, var. time, var. concentrations;
DOI:10.1246/bcsj.54.1571

Reference yield:

: 17213-01-3
sodium anthracene-9-sulfonate

: 116115-32-3
N^α-1-(4-Biphenylyl)-1-methylethoxycarbonyl-N^ω-(9-anthracenesulfonyl)-L-arginine dicyclohexylamine salt

Guidance literature:: Multi-step reaction with 5 steps

1: 44 percent / PCl₃ / 17 h / Heating

2: 1.) 3 M aq. NaOH / 1.) acetone, 0 deg C, 2.) 25 deg C, 2 h

3: TFA / 0.08 h

4: 1.) Triton B, 2.) Et₃N / 1.) MeOH, 2.) DMF, 40 deg C, 1 h

5: silica gel / methanol; CH₂Cl₂

With sodium hydroxide; silica gel; N-benzyl-trimethylammonium hydroxide; triethylamine; trifluoroacetic acid; phosphorus trichloride; In methanol; dichloromethane;
DOI:10.1055/s-1988-27457