2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-

Base Information

Chemical Name:2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-
CAS No.:57606-04-9
Molecular Formula:C₇H₁₂O₃
Molecular Weight:144.17
Hs Code.:
DSSTox Substance ID:DTXSID501019855
Nikkaji Number:J2.363.475I
Wikidata:Q105270434

Synonyms:UDNSVMRLHHBYOK-UHFFFAOYSA-N;DTXSID501019855;57606-04-9;2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-

Suppliers and Price of 2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-

Chemical Property:

PSA：0.00000
LogP:0.00000
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:144.078644241
Heavy Atom Count:10
Complexity:155

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC1(COC(=O)C1O)C

Technology Process of 2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl-

There total 15 articles about 2(3H)-Furanone, 4-ethyldihydro-3-hydroxy-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 134734-34-2,134734-36-4
p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

: 39748-50-0,57606-04-9,108865-89-0,134780-01-1
erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: With lithium hydroxide; In methanol; water; for 0.166667h; Ambient temperature;
DOI:10.1002/jhet.5570280315

Reference yield:

: 134936-48-4
3-Ethyl-2,3-dihydro-furan-3-carboxylic acid methyl ester

: 39748-50-0,57606-04-9,108865-89-0,134780-01-1
erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: Multi-step reaction with 8 steps

1: m-chloroperbenzoic acid / 1 h / 0 °C

2: pyridine / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

4: 61 percent / pyridine / Ambient temperature

5: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

6: 97 percent / pyridine / Ambient temperature

7: 90 percent / BF₃*Et₂O, MCPBA / CH₂Cl₂ / 3 h / Ambient temperature

8: 94 percent / LiOH / methanol; H₂O / 0.17 h / Ambient temperature

With pyridine; lithium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/jhet.5570280315

Reference yield:

: methyl 4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-carboxylate

: 39748-50-0,57606-04-9,108865-89-0,134780-01-1
erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / Ambient temperature

2: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 61 percent / pyridine / Ambient temperature

4: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

5: 97 percent / pyridine / Ambient temperature

6: 90 percent / BF₃*Et₂O, MCPBA / CH₂Cl₂ / 3 h / Ambient temperature

7: 94 percent / LiOH / methanol; H₂O / 0.17 h / Ambient temperature

With pyridine; lithium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/jhet.5570280315