(S)-(+)-3-METHYLPIPERIDINE

Base Information

• Chemical Name: (S)-(+)-3-METHYLPIPERIDINE
• CAS No.: 17305-22-5
• Molecular Formula: C6H13N
• Molecular Weight: 99.1759
• Mol file: 17305-22-5.mol

Synonyms:(S)-3-Chloro-1,2-propanediol;(2S)-3-Chloro-1,2-propanediol;(S)-1,2-chloropropanediol;(S)-3-chloropropane-1,2-diol;(S)-3-Methyl-piperidin;(S)-1-chloro-2,3-dihydroxypropane;1,2-Propanediol,3-chloro-,(S);(S)-chloropropane-2,3-diol;

Chemical Property of (S)-(+)-3-METHYLPIPERIDINE

Chemical Property:

• Boiling Point: 126℃
• PKA: 10.49±0.10(Predicted)
• Flash Point: 17℃
• PSA: 12.03000
• Density: 0.809±0.06 g/cm3(Predicted)
• LogP: 1.33470

Purity/Quality:

97% ^*data from raw suppliers

(S)-(+)-3-Methyl-piperidine >98%ee,>98 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-(+)-3-METHYLPIPERIDINE

There total 5 articles about (S)-(+)-3-METHYLPIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2,5-dioxopyrrolidin-1-yl (R)-2-phenoxypropanoate + 3-Methylpiperidine (626-56-2,53152-98-0) → (R,R)-3-methyl-1-(2-phenoxypropanoyl)piperidine + (R)-3-methyl-1-(2-phenoxypropanoyl)piperidine + (-)-(R)-3-methylpiperidine (16078-25-4) + (+)-(S)-3-methylpiperidine (17305-22-5)

Guidance literature:

In toluene; for 24h; stereoselective reaction;

DOI:10.1039/d1ob02099d

Reference yield: 56.0%

→ 6(R,S)-(3,4-Difluorophenyl)-1,6-dihydro-5-methoxycarbonyl-1-(5-(4-methoxycarbonyl-4-phenylpiperidin-1-yl)-4(S)-methyl)pentyl-2,4-dimethylpyrimidine + (+)-(S)-3-methylpiperidine (17305-22-5)

Guidance literature:

Reference yield:

(S)-4-isopropyl-3-(5-methylpyridin-2-yl)oxazolidin-2-one (737760-90-6) → (4S)-4-isopropyl-1,3-oxazolidin-2-one (17016-83-0) + (+)-(S)-3-methylpiperidine (17305-22-5)

Guidance literature:

With hydrogenchloride; hydrogen; platinum(IV) oxide; In ethanol; water; under 75007.5 Torr;

upstream raw materials:

(S)-4-isopropyl-3-(5-methylpyridin-2-yl)oxazolidin-2-one

2-methylcadaverine

3-Methylpiperidine

Downstream raw materials:

(+)-(S)-N-benzoyl-3-methylpiperidine

(-)-(R)-N-benzoyl-3-methylpiperidine

4-((3-methylpiperidin-1-yl)sulfonyl)aniline

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