2-Butenoic acid, octyl ester, (2E)-

Base Information

• Chemical Name: 2-Butenoic acid, octyl ester, (2E)-
• CAS No.: 173605-13-5
• Molecular Formula: C12H22O2
• Molecular Weight: 0.00000
• Mol file: 173605-13-5.mol

Synonyms:

Chemical Property of 2-Butenoic acid, octyl ester, (2E)-

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Butenoic acid, octyl ester, (2E)-

There total 6 articles about 2-Butenoic acid, octyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

octanol (111-87-5) + (E)-but-2-enoic acid (107-93-7) → 1-octyl 2-butenoate (173605-13-5)

Guidance literature:

With dmap; trimethylamine hydrochloride; triethylamine; dimethylamino sulfonyl chloride; In acetonitrile; at 0 - 5 ℃; for 3h;

DOI:10.1016/S0040-4020(03)00734-8

Reference yield: 55.0%

2-butenoic acid (3724-65-0) + octanol (111-87-5) → but-2-enoic acid octyl ester (22874-79-9,173605-13-5)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c4ra15975f

Reference yield:

octanol (111-87-5) + (E)-but-2-enoic acid (107-93-7) → but-2-enoic acid octyl ester (22874-79-9,173605-13-5)

Guidance literature:

With sodium tetrahydroborate; In toluene; at 120 - 130 ℃; Dean-Stark;

upstream raw materials:

octanol

(E)-but-2-enoic acid

2-butenoic acid