Carbamic acid, [2-[phenyl[[2,3,4,5-tetrahydro-2,4-dioxo-5-phenyl-3-[[(phenylamino)carb onyl]amino]-1H-1,5-benzodiazepin-1-yl]acetyl]amino]ethyl]-, phenylmethyl ester

Base Information

• Chemical Name: Carbamic acid, [2-[phenyl[[2,3,4,5-tetrahydro-2,4-dioxo-5-phenyl-3-[[(phenylamino)carb onyl]amino]-1H-1,5-benzodiazepin-1-yl]acetyl]amino]ethyl]-, phenylmethyl ester
• CAS No.: 173908-74-2
• Molecular Formula: C40H36N6O6
• Molecular Weight: 696.762

Synonyms:

Chemical Property of Carbamic acid, [2-[phenyl[[2,3,4,5-tetrahydro-2,4-dioxo-5-phenyl-3-[[(phenylamino)carb onyl]amino]-1H-1,5-benzodiazepin-1-yl]acetyl]amino]ethyl]-, phenylmethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [2-[phenyl[[2,3,4,5-tetrahydro-2,4-dioxo-5-phenyl-3-[[(phenylamino)carb onyl]amino]-1H-1,5-benzodiazepin-1-yl]acetyl]amino]ethyl]-, phenylmethyl ester

There total 8 articles about Carbamic acid, [2-[phenyl[[2,3,4,5-tetrahydro-2,4-dioxo-5-phenyl-3-[[(phenylamino)carb onyl]amino]-1H-1,5-benzodiazepin-1-yl]acetyl]amino]ethyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl (2-(phenylamino)ethyl)carbamate (101288-83-9) → [2-({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-ethyl]-carbamic acid benzyl ester (173908-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; triethylamine; In dichloromethane;

DOI:10.1021/jm950626d

Reference yield:

phenyl isocyanate (103-71-9) → [2-({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-ethyl]-carbamic acid benzyl ester (173908-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; In dichloromethane;

DOI:10.1021/jm950626d

Reference yield:

3-amino-1-phenyl-1,5-dihydrobenzo<1,4>diazepine-2,4-dione (153930-38-2) → [2-({2-[2,4-Dioxo-5-phenyl-3-(3-phenyl-ureido)-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl]-acetyl}-phenyl-amino)-ethyl]-carbamic acid benzyl ester (173908-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, RT, 16 h

With sodium hydride; In dichloromethane;

DOI:10.1021/jm950626d

upstream raw materials:

benzyl (2-(phenylamino)ethyl)carbamate

phenyl isocyanate

3-amino-1-phenyl-1,5-dihydrobenzo<1,4>diazepine-2,4-dione

N-(4-methoxybenzyl)-N-phenylbenzene-1,2-diamine

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