Propanedioic acid, [(4-chlorophenyl)methylene]-

Base Information

Chemical Name:Propanedioic acid, [(4-chlorophenyl)methylene]-
CAS No.:17449-02-4
Molecular Formula:C10H7ClO4
Molecular Weight:226.616
Hs Code.:

Synonyms:

Suppliers and Price of Propanedioic acid, [(4-chlorophenyl)methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Propanedioic acid, [(4-chlorophenyl)methylene]-

Chemical Property:

Melting Point:197-198 °C (decomp)
Boiling Point:421.5±35.0 °C(Predicted)
PSA：0.00000
Density:1.531±0.06 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Propanedioic acid, [(4-chlorophenyl)methylene]-

There total 5 articles about Propanedioic acid, [(4-chlorophenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 141-82-2
malonic acid

: 104-88-1
4-chlorobenzaldehyde

: 17449-02-4
p-chlorobenzylidenepropane-1,3-dioic acid

Guidance literature:: ytterbium(III) perfluorooctanesulfonate; In toluene; at 80 ℃; for 8h;
DOI:10.1080/00304940709458582

Reference yield: 76.0%

: 141-82-2
malonic acid

: 100-52-7
benzaldehyde

: 17449-02-4
p-chlorobenzylidenepropane-1,3-dioic acid

Guidance literature:: With 2,6-diaminocaproic acid; In ethanol; at 100 ℃; for 2h; Reagent/catalyst;
DOI:10.14233/ajchem.2014.17949

Reference yield:

: 141-82-2
malonic acid

: 104-88-1
4-chlorobenzaldehyde

: 1615-02-7,940-62-5
p-chlorocinnamic acid

: 17449-02-4
p-chlorobenzylidenepropane-1,3-dioic acid

Guidance literature:: 4-chlorobenzaldehyde; With pyridine; (R)-methyl 3-phenyl-2-(3-(pyridin-2-yl)ureido)propanoate; In water; at 20 ℃; for 0.25h;

malonic acid; In water; at 20 ℃; for 6h; Overall yield = 89 %;
DOI:10.1016/j.tetlet.2013.07.116