Benzenemethanol, a-(3,3-dimethyl-1-butynyl)-

Base Information

Chemical Name:Benzenemethanol, a-(3,3-dimethyl-1-butynyl)-
CAS No.:17474-12-3
Molecular Formula:C13H16O
Molecular Weight:188.269
Hs Code.:

Synonyms:4,4-dimethyl-1-hydroxy-1-phenyl-2-pentyne;4,4-Dimethyl-1-phenyl-pent-2-yn-1-ol;1-phenyl-4,4-dimethyl-2-pentyn-1-ol;4,4-dimethyl-1-phenyl-2-pentyn-1-ol;4,4-dimethyl-1-phenylpent-2-yn-1-ol;

Suppliers and Price of Benzenemethanol, a-(3,3-dimethyl-1-butynyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, a-(3,3-dimethyl-1-butynyl)-

Chemical Property:

Boiling Point:73 - 75 °C (0.001 mmHg)
PSA：20.23000
Density:1.010±0.06 g/cm3(Predicted)
LogP:2.76950

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, a-(3,3-dimethyl-1-butynyl)-

There total 7 articles about Benzenemethanol, a-(3,3-dimethyl-1-butynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 66530-03-8
(3,3-dimethylbut-1-ynyl)dimethylaluminium

: 100-52-7
benzaldehyde

: 17474-12-3
4,4-dimethyl-1-phenyl-pent-2-yn-1-ol

Guidance literature:: In n-heptane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/adsc.200900414

Reference yield: 93.0%

: 917-92-0
3,3-Dimethylbut-1-yne

: 100-52-7
benzaldehyde

: 17474-12-3
4,4-dimethyl-1-phenyl-pent-2-yn-1-ol

Guidance literature:: 3,3-Dimethylbut-1-yne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/acs.joc.1c02685