NSC57663

Base Information

• Chemical Name: NSC57663
• CAS No.: 6632-37-7
• Molecular Formula: C14H14 N2 O
• Molecular Weight: 226.278
• Hs Code.: 2924299090
• Mol file: 6632-37-7.mol

Synonyms:Benzanilide,2-amino-N-methyl- (6CI,7CI,8CI); NSC 57663

Chemical Property of NSC57663

Chemical Property:

• Vapor Pressure: 8.57E-07mmHg at 25°C
• Boiling Point: 405.7°C at 760 mmHg
• Flash Point: 199.2°C
• PSA: 46.33000
• Density: 1.196g/cm³
• LogP: 3.12660

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-N-methyl-N-phenylbenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of NSC57663

There total 6 articles about NSC57663 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) + N-methylaniline (100-61-8) → 2-amino-N-methyl-N-phenylbenzamide (6632-37-7)

Guidance literature:

With cetyltrimethylammonim bromide; O,O-Diethyl hydrogen phosphorodithioate; In toluene; for 17h; Heating;

Reference yield: 14.0%

N-methylaniline (100-61-8) + 2-(trifluoromethyl)benzenamine (88-17-5) → 2-amino-N-methyl-N-phenylbenzamide (6632-37-7)

Guidance literature:

With water; sodium hydroxide; In 1,4-dioxane; at 195 ℃; for 6h; Microwave irradiation;

DOI:10.1021/ol100507n

Reference yield:

N-methylaniline (100-61-8) + 2-aminobenzoyl chloride (21563-73-5) → 2-amino-N-methyl-N-phenylbenzamide (6632-37-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/anie.201402925

upstream raw materials:

isatoic anhydride

N-methylaniline

N-methyl-N-phenyl-2-nitrobenzamide

anthranilic acid

Downstream raw materials:

o-aminobenzaldehyde

tert-butyl (2-(methyl(phenyl)carbamoyl)phenyl)carbamate

2-benzamido-N-methyl-N-phenylbenzamide

3-phenyl-4(3H)-quinazolinone

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