Technology Process of Pyrimidine, 2-(3-nitrophenoxy)-
There total 3 articles about Pyrimidine, 2-(3-nitrophenoxy)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dodecacarbonyl-triangulo-triruthenium; copper(II) nitrate trihydrate; silver trifluoroacetate; acetic acid; bis-[(trifluoroacetoxy)iodo]benzene;
In
1,2-dichloro-ethane;
at 100 ℃;
for 28h;
regioselective reaction;
Glovebox;
DOI:10.1039/d0cc02851g
- Guidance literature:
-
With
caesium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / dimethyl sulfoxide / 24 h / 90 °C
2: copper(II) nitrate trihydrate; dodecacarbonyl-triangulo-triruthenium; acetic acid; bis-[(trifluoroacetoxy)iodo]benzene; silver trifluoroacetate / 1,2-dichloro-ethane / 28 h / 100 °C / Glovebox
With
2-Picolinic acid; potassium phosphate; copper(l) iodide; dodecacarbonyl-triangulo-triruthenium; copper(II) nitrate trihydrate; silver trifluoroacetate; acetic acid; bis-[(trifluoroacetoxy)iodo]benzene;
In
dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1039/d0cc02851g