2l2-1,3,2-Benzodioxastannole

Base Information

Chemical Name:2l2-1,3,2-Benzodioxastannole
CAS No.:1767-80-2
Molecular Formula:C₆H₄O₂Sn
Molecular Weight:226.807
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2l2-1,3,2-Benzodioxastannole

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2l2-1,3,2-Benzodioxastannole

There total 4 articles about 2l2-1,3,2-Benzodioxastannole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 7440-31-5
tin

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 1767-80-2
(ortho-phenylenedioxy)stannylene

Guidance literature:: With N(C₂H₅)4⁽¹⁺⁾*ClO₄^(1-); In acetonitrile; byproducts: H2; Electrolysis; Anode: tin rod, cathode: platinum wire coil; 2h.; Filtration, washing with acetonitrile, diethyl ether, drying in vacuo. Identified by elem. anal., NMR, IR.;

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: tin(ll) chloride

: 1767-80-2
(ortho-phenylenedioxy)stannylene

Guidance literature:: With methanol; triethylamine; prepared according to: W.D.Honnic, J.J.Zuckerman, Inorg. Chem., 17, 501 (1978);
DOI:10.1246/bcsj.70.2301