2-cyclopentanone tosylhydrazone

Base Information

• Chemical Name: 2-cyclopentanone tosylhydrazone
• CAS No.: 90862-77-4
• Molecular Formula: C₂₉H₃₂N₂O₂S
• Molecular Weight: 472.651

Synonyms:

Chemical Property of 2-cyclopentanone tosylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-cyclopentanone tosylhydrazone

There total 2 articles about 2-cyclopentanone tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 1,4-dioxaspiro[4,4]nonane-6-carboxylate (23153-73-3) → 2-cyclopentanone tosylhydrazone (90862-77-4)

Guidance literature:

Reference yield:

3,5-dimethyphenylmagnesium bromide (34696-73-6) → 2-cyclopentanone tosylhydrazone (90862-77-4)

Guidance literature:

Reference yield:

2-cyclopentanone tosylhydrazone (90862-77-4) → 1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine (90862-87-6)

Guidance literature:

With sodium ethanolate; Yield given. Multistep reaction; 1.) ethanol, 1 h, in the dark, 2.) reflux;

upstream raw materials:

ethyl 1,4-dioxaspiro[4,4]nonane-6-carboxylate

3,5-dimethyphenylmagnesium bromide

Downstream raw materials:

1,2,3,3a-tetrahydro-6,8-dimethyl-10-(3,5-dimethylphenyl)benzocyclopenta<8><1,2>diazepine

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