Diethyl P-(hydrazinylphenylmethyl)phosphonate

Base Information

Chemical Name:Diethyl P-(hydrazinylphenylmethyl)phosphonate
CAS No.:177720-01-3
Molecular Formula:C11H19N2O3P
Molecular Weight:258.257
Hs Code.:
DSSTox Substance ID:DTXSID501251865
Nikkaji Number:J719.193F

Synonyms:Diethyl P-(hydrazinylphenylmethyl)phosphonate;DTXSID501251865;177720-01-3

Suppliers and Price of Diethyl P-(hydrazinylphenylmethyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl P-(hydrazinylphenylmethyl)phosphonate

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:258.11332947
Heavy Atom Count:17
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(=O)(C(C1=CC=CC=C1)NN)OCC

Technology Process of Diethyl P-(hydrazinylphenylmethyl)phosphonate

There total 3 articles about Diethyl P-(hydrazinylphenylmethyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 51761-45-6,85166-93-4,85166-94-5
Methanesulfonic acid (diethoxy-phosphoryl)-phenyl-methyl ester

: 177720-01-3
diethyl 1-hydroazinobenzylphosphonate

Guidance literature:: With hydrazine hydrate; In ethanol; at 50 ℃; for 15h;
DOI:10.1055/s-1996-4242

Reference yield:

: 100-52-7
benzaldehyde

: 177720-01-3
diethyl 1-hydroazinobenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) Et₃N / 1.) 75 deg C, 30 min, 2.) CH₂Cl₂, RT, 2 h

2: 55 percent / hydrazine hydrate / ethanol / 15 h / 50 °C

With hydrazine hydrate; triethylamine; In ethanol;
DOI:10.1055/s-1996-4242