PHENYLSULFONYLMETHANAL O-BENZYL OXIME

Base Information

Chemical Name:PHENYLSULFONYLMETHANAL O-BENZYL OXIME
CAS No.:177750-79-7
Molecular Formula:C14H13NO3S
Molecular Weight:275.328
Hs Code.:
Mol file:177750-79-7.mol

Synonyms:phenylsulfonylmethanal O-benzyl oxime;N-benzyloxy-1-(phenylsulfonyl)methanimine;Methanimine,N-(phenylmethoxy)-1-(phenylsulfonyl);

Suppliers and Price of PHENYLSULFONYLMETHANAL O-BENZYL OXIME

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PHENYLSULFONYLMETHANAL O-BENZYL OXIME 95.00%
10G
$ 3176.25

American Custom Chemicals Corporation
PHENYLSULFONYLMETHANAL O-BENZYL OXIME 95.00%
1G
$ 1097.25

Total 1 raw suppliers

Chemical Property of PHENYLSULFONYLMETHANAL O-BENZYL OXIME

Chemical Property:

PSA：64.11000
LogP:3.70120

Purity/Quality:: PHENYLSULFONYLMETHANAL O-BENZYL OXIME 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of PHENYLSULFONYLMETHANAL O-BENZYL OXIME

There total 3 articles about PHENYLSULFONYLMETHANAL O-BENZYL OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 177750-77-5
phenyl N-(benzyloxy)methanimidothioate

: 177750-79-7
N-benzyloxy-1-(phenylsulfonyl)methanimine

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 40 ℃; for 1.25h;
DOI:10.3762/bjoc.14.201

Reference yield:

: 72399-18-9
formaldehyde O-benzyloxime

: 177750-79-7
N-benzyloxy-1-(phenylsulfonyl)methanimine

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NCS / dimethylformamide / 3 h / 40 °C

2: 90 percent / tetrahydrofuran / 3 h / 25 °C

3: 88 percent / MCPBA, NaHCO₃ / CH₂Cl₂ / 2 h / 40 °C

With N-chloro-succinimide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja9600993

Reference yield:

: 151451-59-1
N-benzyloxyformhydroxamic chloride

: 177750-79-7
N-benzyloxy-1-(phenylsulfonyl)methanimine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 3 h / 25 °C

2: 88 percent / MCPBA, NaHCO₃ / CH₂Cl₂ / 2 h / 40 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja9600993