di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate

Base Information

• Chemical Name: di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate
• CAS No.: 161896-55-5
• Molecular Formula: C₂H₆OS*C₂₄H₁₆N₄O₆Pd
• Molecular Weight: 640.969
• Mol file: 161896-55-5.mol

Synonyms:

Chemical Property of di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate

There total 1 articles about di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bathophenanthroline (1662-01-7) + nitric acid (7697-37-2,78989-43-2) + palladium (7440-05-3) → di(nitrato-O)(4,7-diphenyl-1,10-phenanthroline-N,N')palladium(II) dimethyl sulfoxide solvate (161896-55-5)

Guidance literature:

Pd soln. in warm HNO3, phenanthroline addn. (4:1 ratio), evapn. to 1/4 volume, cooling. (pptn.), soln. (dimethylformamide/dimethyl sulfoxide = 1:1); crystn. (solvent evapn. in N2-stream);

DOI:10.1107/S0108270194008887

upstream raw materials:

bathophenanthroline

nitric acid

palladium