1-Chloro-4-nitro-2-(phenylmethyl)benzene

Base Information

Chemical Name:1-Chloro-4-nitro-2-(phenylmethyl)benzene
CAS No.:178678-21-2
Molecular Formula:C13H10ClNO2
Molecular Weight:247.681
Hs Code.:
DSSTox Substance ID:DTXSID301274489
Mol file:178678-21-2.mol

Synonyms:1-Chloro-4-nitro-2-(phenylmethyl)benzene;SCHEMBL6203707;DTXSID301274489;178678-21-2

Suppliers and Price of 1-Chloro-4-nitro-2-(phenylmethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Chloro-4-nitro-2-(phenylmethyl)benzene

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:247.0400063
Heavy Atom Count:17
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC2=C(C=CC(=C2)[N+](=O)[O-])Cl

Technology Process of 1-Chloro-4-nitro-2-(phenylmethyl)benzene

There total 1 articles about 1-Chloro-4-nitro-2-(phenylmethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 34052-37-4
2-chloro-5-nitrobenzophenone

: 178678-21-2
2-chloro-5-nitrodiphenylmethane

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane;
DOI:10.1021/jm040215+

Reference yield:

: 178678-21-2
2-chloro-5-nitrodiphenylmethane

: 2-benzyl-4-nitro-benzenethiol

Guidance literature:: With lithium sulfide; In dimethyl sulfoxide; at 75 ℃; for 15h;
DOI:10.1021/jm040215+

Reference yield:

: 178678-21-2
2-chloro-5-nitrodiphenylmethane

: 3-(4-amino-2-benzyl-benzenesulfonyl)-2,2-dimethyl-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: Li₂S / dimethylsulfoxide / 15 h / 75 °C

2: Et₃N / various solvent(s) / Heating

3: mCPBA / CH₂Cl₂

4: H₂ / Pd/C / CH₂Cl₂ / 5171.48 Torr

With lithium sulfide; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm040215+