Decyl(phenyl)silane

Base Information

• Chemical Name: Decyl(phenyl)silane
• CAS No.: 17897-66-4
• Molecular Formula: C16H28Si
• Molecular Weight: 248.484
• DSSTox Substance ID: DTXSID10400476
• Mol file: 17897-66-4.mol

Synonyms:decyl(phenyl)silane;17897-66-4;DTXSID10400476

Chemical Property of Decyl(phenyl)silane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 10
• Exact Mass: 246.180377364
• Heavy Atom Count: 17
• Complexity: 150

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCC[Si]C1=CC=CC=C1

Technology Process of Decyl(phenyl)silane

There total 7 articles about Decyl(phenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

phenylchlorosilane (4206-75-1) → 1-(phenylsilyl)decane (17897-66-4)

Guidance literature:

In tetrahydrofuran; diethyl ether; at 30 ℃;

DOI:10.1039/b717717h

Reference yield: 98.0%

phenylchlorosilane (4206-75-1) + n-decyl magnesium bromide (17049-50-2) → 1-(phenylsilyl)decane (17897-66-4)

Guidance literature:

In diethyl ether; at 30 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja206745w

Reference yield: 41.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) + phenylsilane (694-53-1) → C26H48Si + 1-(phenylsilyl)decane (17897-66-4)

Guidance literature:

With THF coordination iron oxide nanoparticles; In tetrahydrofuran; at 60 ℃; for 24h; Reagent/catalyst; Temperature; Solvent; Concentration; Schlenk technique; Inert atmosphere;

upstream raw materials:

phenylsilane

n-decyl magnesium bromide

1-Decene

1-decyne