Technology Process of Krypton difluoride
There total 8 articles about Krypton difluoride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent);
electrical discharge at -183 to - 196°C and 20 Torr pressure; typical conditions: F2-Kr-mixture (1.1:1) at 20 Torr and -196°C, electrical discharge of 20 mA and 3000-4000 V;; at typical conditions, 0.25g KrF2/h are obtained; sublimation of raw product below 0°C; careful drying in a pre-fluorinated apparatus;;
DOI:10.1021/ja01079a006
- Guidance literature:
-
In
neat (no solvent);
high frequency electrical discharge in F2-CF2Cl2 mixtures; circulation of react. mixture; using of a cooled quartz apparatus, electrodes at the outer side of walls;;
