p-tolyltriethylphosphonium hexafluorophosphate

Base Information

• Chemical Name: p-tolyltriethylphosphonium hexafluorophosphate
• CAS No.: 137161-92-3
• Molecular Formula: C₁₃H₂₂P*F₆P
• Molecular Weight: 354.256
• Mol file: 137161-92-3.mol

Synonyms:

Chemical Property of p-tolyltriethylphosphonium hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of p-tolyltriethylphosphonium hexafluorophosphate

There total 1 articles about p-tolyltriethylphosphonium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tricarbonyl(η(6)-4-chlorotoluene)manganese hexafluorophosphate (57813-15-7) + triethylphosphine (554-70-1) → fac-{Cl(triethylphosphine)2tricarbonylmanganese} (137172-03-3) + p-tolyltriethylphosphonium hexafluorophosphate (137161-92-3)

Guidance literature:

In acetone; addn. of PEt3 to the Mn compd. in acetone at room temp. under N2 and react. for 2 min; pptn. of the phosphonium salt, filtn., evapn. of the filtrate and recrystn. from n-pentane at -78°C;

DOI:10.1016/0022-328X(91)80052-L

upstream raw materials:

tricarbonyl(η(6)-4-chlorotoluene)manganese hexafluorophosphate

triethylphosphine