1,5-Naphthalenediamine, N,N,N',N'-tetramethyl-

Base Information

• Chemical Name: 1,5-Naphthalenediamine, N,N,N',N'-tetramethyl-
• CAS No.: 10075-69-1
• Molecular Formula: C14H18 N2
• Molecular Weight: 214.31
• DSSTox Substance ID: DTXSID00143486
• Nikkaji Number: J1.964.648C
• Wikidata: Q83007370
• Mol file: 10075-69-1.mol

Synonyms:10075-69-1;N1,N1,N5,N5-Tetramethylnaphthalene-1,5-diamine;1-N,1-N,5-N,5-N-tetramethylnaphthalene-1,5-diamine;1,5-Naphthalenediamine, N,N,N',N'-tetramethyl-;1,5-Naphthalenediamine, N1,N1,N5,N5-tetramethyl-;1,5-Bis(dimethylamino)naphthalene;1,5-Naphthalenediamine,N,N,N',N'-tetramethyl-;SCHEMBL8720110;DTXSID00143486

Chemical Property of 1,5-Naphthalenediamine, N,N,N',N'-tetramethyl-

Chemical Property:

• Boiling Point: 304.4oC at 760 mmHg
• Flash Point: 128.3oC
• PSA: 6.48000
• Density: 1.074g/cm3
• LogP: 2.97180
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 214.146998583
• Heavy Atom Count: 16
• Complexity: 201

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=CC2=C1C=CC=C2N(C)C

Technology Process of 1,5-Naphthalenediamine, N,N,N',N'-tetramethyl-

There total 7 articles about 1,5-Naphthalenediamine, N,N,N',N'-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,5-naphthalenediamine (2243-62-1) → N1,N1,N5,N5-tetramethyl-1,5-diaminonaphthalene (10075-69-1)

Guidance literature:

formaldehyd; 1,5-naphthalenediamine; In ethanol; water;

With platinum(IV) oxide; hydrogen; In ethanol; water; under 760.051 Torr;

DOI:10.1016/j.tet.2016.02.002

Reference yield: 94.7%

dimethyl sulfate (77-78-1) + 1,5-naphthalenediamine (2243-62-1) → N1,N1,N5,N5-tetramethyl-1,5-diaminonaphthalene (10075-69-1)

Guidance literature:

With sodium carbonate; In methanol; for 5h;

DOI:10.1021/je060394v

Reference yield: 84.0%

1,5-naphthalenediamine (2243-62-1) + methyl iodide (74-88-4) → N1,N1,N5,N5-tetramethyl-1,5-diaminonaphthalene (10075-69-1)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1023/A:1019615206870

upstream raw materials:

dimethyl sulfate

1,5-naphthalenediamine

trimethyl phosphite

methyl iodide

Downstream raw materials:

4,8-bis-diphenylphosphanyl-N,N,N',N'-tetramethyl-naphthalene-1,5-diamine