hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II)

Base Information

Chemical Name:hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II)
CAS No.:82285-08-3
Molecular Formula:C₆H₁₅Cl₃PPt*C₉H₁₇N₂
Molecular Weight:572.845
Hs Code.:

Synonyms:

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Chemical Property of hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II)

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Technology Process of hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II)

There total 1 articles about hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: dichloro-bis(triethylphosphine)-di-μ-chloro-diplatinum(II)

: 67565-91-7
mesityldiphenylmethylenephoshine

: 6674-22-2,83329-50-4
1,8-diazabicyclo[5.4.0]undec-7-ene

: 78777-26-1,78822-10-3
cis dichloro(triethylphosphine)(P-mesityl diphenylmethylene phosphine)platinum(II)

: 78822-10-3,78777-26-1
trans-PtCl₂(PEt₃)(P(mesityl)=CPh₂)

: 82285-08-3
hydro-1,5-diazabicyclo[5,4,0]-undec-1-ene trichloro(triethylphosphine)platinate(II)

Guidance literature:: In dichloromethane; under N2 or vac.; Pt2Cl4(P(Et3)2 in THF was stirred for 1 h at room temp. with (mesityl)P=CPh2 to produce a soln. of trans-PtCl2(PEt2)(P(mesityl)=CPh2); removal of solvent produced an oil which was stirred with hexane to produce the cis isomer; crystn. from CH2Cl2/hexane yielded (DBUH)(PtCl3(P(C2H5)3); elem. anal.;
DOI:10.1016/S0277-5387(00)81074-8