2-Benzoyl-4-methylpyridine

Base Information

Chemical Name:2-Benzoyl-4-methylpyridine
CAS No.:18103-77-0
Molecular Formula:C13H11NO
Molecular Weight:197.236
Hs Code.:
DSSTox Substance ID:DTXSID20393345
Nikkaji Number:J2.012.860G
Wikidata:Q82192096
Mol file:18103-77-0.mol

Synonyms:2-benzoyl-4-methylpyridine;18103-77-0;(4-methylpyridin-2-yl)-phenylmethanone;(4-Methylpyridin-2-yl)(phenyl)methanone;MFCD00666136;DTXSID20393345;AKOS013152345;(4-methyl-2-pyridinyl)(phenyl)methanone

Suppliers and Price of 2-Benzoyl-4-methylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Benzoyl-4-methylpyridine

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:197.084063974
Heavy Atom Count:15
Complexity:221

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NC=C1)C(=O)C2=CC=CC=C2

Technology Process of 2-Benzoyl-4-methylpyridine

There total 9 articles about 2-Benzoyl-4-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-89-4
picoline

: 611-74-5
N,N-dimethylbenzamide

: 18103-77-0
(4-methylpyridin-2-yl)(phenyl)methanone

Guidance literature:: picoline; With n-butyllithium; 2-(N,N-dimethylamino)ethanol; In hexane; at 0 ℃; for 1h;

N,N-dimethylbenzamide; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Further stages.;
DOI:10.1002/ejoc.200300243

Reference yield: 78.0%

: 1003-67-4
4-methylpyridine-1-oxide

: 536-74-3
phenylacetylene

: 18103-77-0
(4-methylpyridin-2-yl)(phenyl)methanone

Guidance literature:: With dipotassium peroxodisulfate; water; silver nitrate; at 20 ℃;
DOI:10.1021/acs.joc.8b01475

Reference yield: 73.0%

: 10364-94-0
1-benzoylimidazole

: (4-methylpyridin-2-yl)triphenylphosphonium bromide

: 18103-77-0
(4-methylpyridin-2-yl)(phenyl)methanone

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.orglett.1c02165