1,3,5-Trimethyl-1,3,5-Trisilacyclohexane

Base Information

• Chemical Name: 1,3,5-Trimethyl-1,3,5-Trisilacyclohexane
• CAS No.: 18186-89-5
• Molecular Formula: C6H18Si3
• Molecular Weight: 174.465
• Mol file: 18186-89-5.mol

Synonyms:1,3,5-Trimethyl-[1,3,5]trisilinane;1,3,5-Tris(methylsila)-cyclohexan;1.3.5-Trimethyl-1.3.5-trisilacyclohexan;

Chemical Property of 1,3,5-Trimethyl-1,3,5-Trisilacyclohexane

Chemical Property:

• Melting Point: 32-36°C
• Boiling Point: 60°C / 10
• PSA: 0.00000
• LogP: 1.18830

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-Trimethyl-1,3,5-Trisilacyclohexane

There total 4 articles about 1,3,5-Trimethyl-1,3,5-Trisilacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl(chloromethyl)hydrochlorosilane (20156-51-8) → dimethylmonochlorosilane (1066-35-9) + 1,3,3-Trimethyl-1,3-disilapropan (18148-13-5) + 2,5-disilahexane (4405-22-5) + 1,1,3-trimethyl-1,3-disilacyclobutane (25261-26-1) + (Chloro-methyl-silanyl)-dimethylsilanyl-methane + 1,3,5-trimethyl-[1,3,5]trisilinane (18186-89-5)

Guidance literature:

With potassium Sodium; In gaseous matrix; at 280 - 320 ℃; under 0.1 - 1 Torr; Product distribution; Mechanism; study of reaction of further chloromethylchlorosilanes;

DOI:10.1016/0022-328X(85)87334-4

Reference yield:

1,3,5-trichloro-1,3,5-trimethyl-1,3,5-trisilacyclohexane (1628-02-0) → 1,3,5-trimethyl-[1,3,5]trisilinane (18186-89-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jo01029a081

Reference yield:

1,3,5-triethoxy-1,3,5-trimethyl-1,3,5-trisilacyclohexane (1747-56-4) → 1,3,5-trimethyl-[1,3,5]trisilinane (18186-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₃

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; phosphorus trichloride; In diethyl ether;

DOI:10.1021/jo01029a081

upstream raw materials:

1,3,5-trichloro-1,3,5-trimethyl-1,3,5-trisilacyclohexane

methyl(chloromethyl)hydrochlorosilane

1,3,5-triethoxy-1,3,5-trimethyl-1,3,5-trisilacyclohexane