Cl₂Ru(CDCHCHPh)(PCy₃)2

Base Information

• Chemical Name: Cl₂Ru(CDCHCHPh)(PCy₃)2
• CAS No.: 1215341-66-4
• Molecular Formula: C₄₅H₇₄Cl₂P₂Ru
• Molecular Weight: 849.998
• Mol file: 1215341-66-4.mol

Synonyms:

Chemical Property of Cl₂Ru(CDCHCHPh)(PCy₃)2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Cl₂Ru(CDCHCHPh)(PCy₃)2

There total 2 articles about Cl₂Ru(CDCHCHPh)(PCy₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Grubbs catalyst first generation + water-d2 (7789-20-0) + trimethylsilylacetylene (1066-54-2) → Cl2Ru(CDCHCHPh)(PCy3)2 (1215341-66-4)

Guidance literature:

In not given; byproducts: [(CH3)3Si]2O; treatment ruthenium complex with silicon compd. in the presence of D2O (5 equiv.); NMR;

DOI:10.1039/b924945c

Reference yield:

Grubbs catalyst first generation + deuteromethanol (1455-13-6) + trimethylsilylacetylene (1066-54-2) → Cl2Ru(CDCHCHPh)(PCy3)2 (1215341-66-4)

Guidance literature:

In not given; byproducts: (CH3)3SiOCH3; treatment ruthenium complex with silicon compd. in the presence of CH3OD; NMR;

DOI:10.1039/b924945c

upstream raw materials:

deuteromethanol

trimethylsilylacetylene

water-d2