Technology Process of Pyridine, 2-(2-nitro-1-phenylethenyl)-, (E)-
There total 6 articles about Pyridine, 2-(2-nitro-1-phenylethenyl)-, (E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iodine; sodium nitrite;
In
water; ethylene glycol; ethyl acetate;
at 20 ℃;
for 72h;
DOI:10.1002/jhet.5570330435
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) nBuLi, 3.) 10percent aq. ammonium chloride, 4.) sulfuric acid, gl. acetic acid
2: 30 percent / sodium nitrite, iodine / ethane-1,2-diol; H2O; ethyl acetate / 72 h / 20 °C
With
n-butyllithium; sulfuric acid; ammonium chloride; iodine; acetic acid; sodium nitrite;
In
water; ethylene glycol; ethyl acetate;
DOI:10.1002/jhet.5570330435
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) nBuLi, 3.) 10percent aq. ammonium chloride, 4.) sulfuric acid, gl. acetic acid
2: 30 percent / sodium nitrite, iodine / ethane-1,2-diol; H2O; ethyl acetate / 72 h / 20 °C
With
n-butyllithium; sulfuric acid; ammonium chloride; iodine; acetic acid; sodium nitrite;
In
water; ethylene glycol; ethyl acetate;
DOI:10.1002/jhet.5570330435