phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate

Base Information

• Chemical Name: phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate
• CAS No.: 346731-45-1
• Molecular Formula: BF₄*C₃₆H₄₁N₂OP₂Pd
• Molecular Weight: 772.906
• Mol file: 346731-45-1.mol

Synonyms:

Chemical Property of phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate

There total 4 articles about phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((di-iso-propylphosphino)methyl)-1-methyl-1H-imidazole (230621-88-2) → phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate (346731-45-1)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran

2: acetone

3: dichloromethane-d2

In tetrahydrofuran; dichloromethane-d2; acetone;

DOI:10.1039/b009599k

Reference yield:

iodobenzene (591-50-4) → phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate (346731-45-1)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran

2: acetone

3: dichloromethane-d2

In tetrahydrofuran; dichloromethane-d2; acetone;

DOI:10.1039/b009599k

Reference yield:

phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)palladium(II) tetrafluoroborate (346731-38-2) + carbon monoxide (201230-82-2) → phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)monocarbonylpalladium(II) tetrafluoroborate (346731-45-1)

Guidance literature:

In dichloromethane-d2; under N2; CO gas (1 atm) bubbled through soln. of Pd complex in CD2Cl2 for 10 min; stored at -10°C for 7 d; not isolated; monitored by NMR spectra;

DOI:10.1039/b009599k

upstream raw materials:

phenyl(triphenylphosphine)(2-(diisopropylphosphinomethyl)-1-methylimidazole)palladium(II) tetrafluoroborate

carbon monoxide

2-((di-iso-propylphosphino)methyl)-1-methyl-1H-imidazole

phenyl(2-(diisopropylphosphinomethyl)-1-methylimidazole)iodopalladium(II)