BrAu(μ-Ph2P(CH2)8PPh2)AuBr

Base Information

Chemical Name:BrAu(μ-Ph2P(CH2)8PPh2)AuBr
CAS No.:72476-72-3
Molecular Formula:C₃₂H₃₆Au₂Br₂P₂
Molecular Weight:1036.33
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BrAu(μ-Ph2P(CH2)8PPh2)AuBr

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Technology Process of BrAu(μ-Ph2P(CH2)8PPh2)AuBr

There total 2 articles about BrAu(μ-Ph2P(CH2)8PPh2)AuBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tetraethylammonium dibromoaurate(I)

: 41625-30-3
1,8-bis(diphenylphosphanyl)octane

: 72476-72-3
BrAu(μ-Ph2P(CH2)8PPh2)AuBr

Guidance literature:: In ethanol; dichloromethane; an ethanol soln. of (NEt4)(AuBr2) was added to a CH2Cl2 soln. of ligand under N2 and stirred for 15 min; soln. was then concd., n-pentane was added, ppt. was filtered off, washed with water, dried in vac. over P2O5 at 100°C for 1 d; elem.anal.;

Reference yield:

: 15189-51-2
sodium tetrachloroaurate(III)

: 41625-30-3
1,8-bis(diphenylphosphanyl)octane

: 7550-35-8
lithium bromide

: 72476-72-3
BrAu(μ-Ph2P(CH2)8PPh2)AuBr

Guidance literature:: In not given; treatment of Au-complex with 4-5 equiv. of LiBr, then addn. of equimolaramt. of ligand; elem. anal.;
DOI:10.1039/DT9790001730