(1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide

Base Information

Chemical Name:(1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide
CAS No.:2689-63-6
Molecular Formula:C27H24BrOP
Molecular Weight:475.365
Hs Code.:2931900090
European Community (EC) Number:220-255-3
DSSTox Substance ID:DTXSID20949684
Mol file:2689-63-6.mol

Synonyms:2689-63-6;(alpha-Methylphenacyl)triphenylphosphonium bromide;(1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide;2-(Triphenylphosphonio)propiophenone bromide;(1-Oxo-1-phenylpropan-2-yl)triphenylphosphonium bromide;EINECS 220-255-3;(1-oxo-1-phenylpropan-2-yl)-triphenylphosphanium;bromide;(1-Benzoylethyl)triphenylphosphonium bromide;C27H24OP.Br;SCHEMBL2447096;C27-H24-O-P.Br;DTXSID20949684;BP-12962;FT-0604859;A818666;J-016591;(1-Oxo-1-phenylpropan-2-yl)triphenylphosphoniumbromide;(1-Oxo-1-phenylpropan-2-yl)(triphenyl)phosphanium bromide

Suppliers and Price of (1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(TRIPHENYLPHOSPHONIO)PROPIOPHENONE BROMIDE 95.00%
5G
$ 177.24

Alfa Aesar
2-(Triphenylphosphonio)propiophenone bromide, 98+%
25g
$ 223.00

Alfa Aesar
2-(Triphenylphosphonio)propiophenone bromide, 98+%
5g
$ 59.50

Alfa Aesar
2-(Triphenylphosphonio)propiophenone bromide, 98+%
100g
$ 792.00

AHH
(alpha-Methylphenacyl)triphenylphosphoniumbromide 98%
100g
$ 255.00

Total 20 raw suppliers

Chemical Property of (1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide

Chemical Property:

Melting Point:244-246oC
PSA：30.66000
LogP:2.25590
Sensitive.:Hygroscopic
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:474.07481
Heavy Atom Count:30
Complexity:459

Purity/Quality:

97% ^*data from raw suppliers

2-(TRIPHENYLPHOSPHONIO)PROPIOPHENONE BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=O)C1=CC=CC=C1)[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[Br-]

Technology Process of (1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide

There total 3 articles about (1-Methyl-2-oxo-2-phenylethyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2114-00-3
2-bromo-1-phenyl-1-propanone

: 603-35-0
triphenylphosphine

: 2689-63-6
1-benzoylethylidenephosphonium bromide

Guidance literature:: In benzene; for 24h; Heating;
DOI:10.1080/07328309808002357

Reference yield:

: 93-55-0
1-phenyl-propan-1-one

: 2689-63-6
1-benzoylethylidenephosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / dichloromethane / 3 h / 20 °C

2: tetrahydrofuran / 4 h / Reflux

With bromine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.8b00612