Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-

Base Information

Chemical Name:Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-
CAS No.:183955-08-0
Molecular Formula:C18H30OSi
Molecular Weight:290.521
Hs Code.:
DSSTox Substance ID:DTXSID60476146
Nikkaji Number:J1.856.801B

Synonyms:Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-;183955-08-0;DTXSID60476146

Suppliers and Price of Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:10
Exact Mass:290.206592111
Heavy Atom Count:20
Complexity:246

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Si](CC)(CC)OC(CCC1=CC=CC=C1)CC=C

Technology Process of Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]-

There total 2 articles about Silane, triethyl[[1-(2-phenylethyl)-3-butenyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 994-30-9
triethylsilyl chloride

: 60340-28-5
1-phenylhex-5-en-3-ol

: 183955-08-0
triethyl((1-phenylhex-5-en-3-yl)oxy)silane

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/ol0271382

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 183955-08-0
triethyl((1-phenylhex-5-en-3-yl)oxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; ammonium chloride / tetrahydrofuran; water / 0.5 h / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; ammonium chloride; zinc; In tetrahydrofuran; dichloromethane; water; 1: |Michael Addition;
DOI:10.1039/C6OB02333A

Reference yield: 100.0%

: 183955-08-0
triethyl((1-phenylhex-5-en-3-yl)oxy)silane

: 5-phenyl-3-((triethylsilyl)oxy)pentanal

Guidance literature:: With ozone; triphenylphosphine; In methanol; dichloromethane; at -78 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1039/C6OB02333A