2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one
CAS No.:18595-87-4
Molecular Formula:C15H11NO2
Molecular Weight:237.258
Hs Code.:
European Community (EC) Number:653-997-5
Nikkaji Number:J575.803C
ChEMBL ID:CHEMBL2360992

Synonyms:2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one;2-o-Tolyl-benzo[d][1,3]oxazin-4-one;Oprea1_369567;Oprea1_833784;MLS001207429;SCHEMBL913682;CHEMBL2360992;BDBM222124;STK057764;AKOS000638334;18595-87-4;SMR000514156;2-(2-tolyl)-4h-3,1-benzoxazin-4-one;2-(o-Tolyl)-4H-benzo[d][1,3]oxazin-4-one;SR-01000887159;SR-01000887159-2;2-(2-Methylphenyl)-4H-3,1-benzoxazin-4-one (13)

Suppliers and Price of 2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:237.078978594
Heavy Atom Count:18
Complexity:364

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C2=NC3=CC=CC=C3C(=O)O2

Technology Process of 2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

There total 25 articles about 2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: N-(2-acetylphenyl)-2-methylbenzamide

: 18595-87-4
2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: N-(2-acetylphenyl)-2-methylbenzamide; With iodine; sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 0.0333333h;

With tert.-butylhydroperoxide; In nonane; dimethyl sulfoxide; at 95 ℃; for 3h;
DOI:10.1021/acs.orglett.6b02142

Reference yield: 84.0%

: 31162-13-7
2-azidobenzoic acid

: 933-88-0
ortho-toluoyl chloride

: 18595-87-4
2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: With 1,1,3,3-Tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate); triethylamine; triphenylphosphine; In toluene; at 110 ℃; Reflux;
DOI:10.1021/acscatal.6b00165

Reference yield: 81.0%

: 6919-61-5
N-methoxy-N-methylbenzamide

: 3-(2-methylphenyl)-1,4,2-dioxazol-5-one

: 18595-87-4
2-(2-methylphenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: With silver hexafluoroantimonate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; acetic anhydride; In 1,2-dichloro-ethane; at 80 ℃; for 18h;
DOI:10.3987/COM-18-S(F)48