trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure

Base Information

• Chemical Name: trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure
• CAS No.: 17081-81-1
• Molecular Formula: C₁₅H₂₁ClO₂
• Molecular Weight: 268.784
• Mol file: 17081-81-1.mol

Synonyms:

Chemical Property of trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure

There total 2 articles about trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one (79-77-6,14901-07-6) → trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure (17081-81-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) PhLi, piperidine, (ii) /BRN= 1909544/

2: (i) nBuLi, (ii) /BRN= 1900390/

DOI:10.1002/jlac.19677040106

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + β-Ionyliden-chlormethan (17081-79-7) → trans-trans-2-Chlor-3-methyl-5-<2,2,6-trimethylcyclohexen-(6)-yl>-pentadien-(2,4)-saeure; 9-trans-10-Chlor-β-jonylidenessigsaeure (17081-81-1)

Guidance literature:

Multistep reaction; (i) nBuLi, (ii) /BRN= 1900390/;

DOI:10.1002/jlac.19677040106

upstream raw materials:

carbon dioxide

β-Ionyliden-chlormethan

4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one