4-Iodo-2,5-dioctyloxybenzaldehyde

Base Information

Chemical Name:4-Iodo-2,5-dioctyloxybenzaldehyde
CAS No.:186358-39-4
Molecular Formula:C23H37IO3
Molecular Weight:488.449
Hs Code.:
DSSTox Substance ID:DTXSID30405362
Nikkaji Number:J1.475.281A
Wikidata:Q82209870

Synonyms:4-iodo-2,5-dioctyloxybenzaldehyde;186358-39-4;ST013926;4-IODO-2,5-BIS(OCTYLOXY)BENZALDEHYDE;DTXSID30405362;AKOS024275785

Suppliers and Price of 4-Iodo-2,5-dioctyloxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Iodo-2,5-dioctyloxybenzaldehyde

Chemical Property:

XLogP3:8.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:17
Exact Mass:488.17874
Heavy Atom Count:27
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCOC1=CC(=C(C=C1C=O)OCCCCCCCC)I

Technology Process of 4-Iodo-2,5-dioctyloxybenzaldehyde

There total 6 articles about 4-Iodo-2,5-dioctyloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5763-87-1
N,N-dimethylvinylamine

: 145483-68-7
1,4-diiodo-2,5-dioctyloxybenzene

: 186358-39-4
4-iodo-2,5-bis-octyloxy-benzaldehyde

Guidance literature:: With n-butyllithium; In diethyl ether; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.5b02542

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 186358-39-4
4-iodo-2,5-bis-octyloxy-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

2: 59 percent / I₂; KIO₃; aq. H₂SO₄ / acetic acid / 24 h / 80 °C

3: 85 percent / BuLi / tetrahydrofuran; diethyl ether / 2.5 h / 0 °C

With potassium iodate; n-butyllithium; sulfuric acid; iodine; potassium carbonate; In tetrahydrofuran; diethyl ether; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200490266

Reference yield:

: 67399-94-4
1,4-bis(octyloxy)benzene

: 186358-39-4
4-iodo-2,5-bis-octyloxy-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / I₂; KIO₃; aq. H₂SO₄ / acetic acid / 24 h / 80 °C

2: 85 percent / BuLi / tetrahydrofuran; diethyl ether / 2.5 h / 0 °C

With potassium iodate; n-butyllithium; sulfuric acid; iodine; In tetrahydrofuran; diethyl ether; acetic acid;
DOI:10.1002/hlca.200490266