Technology Process of C36H31N5O3
There total 8 articles about C36H31N5O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / -20 °C
2: zinc; acetic acid
3: lithium hexamethyldisilazane
4: sodium hydride
5: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / 90 °C
6: trimethylsilyl iodide
With
bis-triphenylphosphine-palladium(II) chloride; 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; trimethylsilyl iodide; sodium hydride; potassium carbonate; acetic acid; lithium hexamethyldisilazane; zinc;
5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.03.109
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / 90 °C
2: trimethylsilyl iodide
With
bis-triphenylphosphine-palladium(II) chloride; trimethylsilyl iodide; potassium carbonate;
1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.03.109
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / -20 °C
2: zinc; acetic acid
3: lithium hexamethyldisilazane
4: sodium hydride
5: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / 90 °C
6: trimethylsilyl iodide
With
bis-triphenylphosphine-palladium(II) chloride; 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; trimethylsilyl iodide; sodium hydride; potassium carbonate; acetic acid; lithium hexamethyldisilazane; zinc;
5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.03.109