Acetic acid, diazo-, 3-phenyl-2-propenyl ester

Base Information

Chemical Name:Acetic acid, diazo-, 3-phenyl-2-propenyl ester
CAS No.:188626-56-4
Molecular Formula:C11H10N2O2
Molecular Weight:202.213
Hs Code.:

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Chemical Property of Acetic acid, diazo-, 3-phenyl-2-propenyl ester

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Technology Process of Acetic acid, diazo-, 3-phenyl-2-propenyl ester

There total 4 articles about Acetic acid, diazo-, 3-phenyl-2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cinnamyl 2-bromoacetate

: 188626-56-4
cinnamyl 2-diazoacetate

Guidance literature:: With N,N'-ditosylhydrazine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 - 20 ℃; for 0.583333h; Sealed tube; Inert atmosphere;
DOI:10.15227/orgsyn.089.0501

Reference yield:

: 104-54-1
3-Phenylpropenol

: 188626-56-4
cinnamyl 2-diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile / 0.92 h / 0 °C / Sealed tube; Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N'-ditosylhydrazine / tetrahydrofuran / 0.58 h / 0 - 20 °C / Sealed tube; Inert atmosphere

With N,N'-ditosylhydrazine; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetonitrile;
DOI:10.15227/orgsyn.089.0501

Reference yield:

: 57582-46-4
cinnamyl 3-oxobutanoate

: 188626-56-4
cinnamyl 2-diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: water; lithium hydroxide / tetrahydrofuran / 6 h / Inert atmosphere

With 4-acetamidobenzenesulfonyl azide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran;
DOI:10.1021/ja2062506