Benzene, 1-(bromoethynyl)-4-iodo-

Base Information

Chemical Name:Benzene, 1-(bromoethynyl)-4-iodo-
CAS No.:1899-09-8
Molecular Formula:C8H4BrI
Molecular Weight:306.928
Hs Code.:
Mol file:1899-09-8.mol

Synonyms:4-(bromoethynyl)iodobenzene;1-iodo-4-(bromoethynyl)benzene;Brom-<4-iod-phenyl>-acetylen;1-(bromoethynyl)-4-iodobenzene;Brom-(4-iod-phenyl)-acetylen;1-(p-Iodphenyl)-2-brom-acetylen;1-Bromoethynyl-4-iodo-benzene;

Suppliers and Price of Benzene, 1-(bromoethynyl)-4-iodo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1-(bromoethynyl)-4-iodo-

Chemical Property:

Melting Point:102 - 104 °C
PSA：0.00000
LogP:2.99510

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, 1-(bromoethynyl)-4-iodo-

There total 6 articles about Benzene, 1-(bromoethynyl)-4-iodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 766-99-4
1-ethynyl-4-iodobenzene

: 1899-09-8
1-(2-bromoethynyl)-4-iodobenzene

Guidance literature:: 1-ethynyl-4-iodobenzene; With silver nitrate; In acetone; for 0.5h;

With N-Bromosuccinimide; In acetone; for 24h; Darkness;
DOI:10.1002/chem.201302162

Reference yield:

: 391198-57-5
[2-(4-iodophenyl)ethynyl]triisopropylsilane

: 1899-09-8
1-(2-bromoethynyl)-4-iodobenzene

Guidance literature:: With N-Bromosuccinimide; silver fluoride; In acetonitrile; at 20 ℃; for 3h; Inert atmosphere; Darkness;
DOI:10.1002/anie.201006879

Reference yield:

: 624-38-4,1032416-46-8
para-diiodobenzene

: 1899-09-8
1-(2-bromoethynyl)-4-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: TurboGrignard / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

1.2: 0.25 h / -78 °C / Inert atmosphere

2.1: N-Bromosuccinimide; silver fluoride / acetonitrile / 3 h / 20 °C / Inert atmosphere; Darkness

With N-Bromosuccinimide; TurboGrignard; silver fluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.201006879