1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-

Base Information

Chemical Name:1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-
CAS No.:630104-26-6
Molecular Formula:C10H14IN3
Molecular Weight:303.146
Hs Code.:
DSSTox Substance ID:DTXSID70451449
Nikkaji Number:J2.240.499G

Synonyms:1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-;630104-26-6;SCHEMBL1754834;SCHEMBL2107414;DTXSID70451449;1-(4-iodophenyl)-3,3-diethyltriazene

Suppliers and Price of 1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:303.02325
Heavy Atom Count:14
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)N=NC1=CC=C(C=C1)I

Technology Process of 1-Triazene, 3,3-diethyl-1-(4-iodophenyl)-

There total 3 articles about 1-Triazene, 3,3-diethyl-1-(4-iodophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 109-89-7
diethylamine

: 540-37-4
p-aminoiodobenzene

: 630104-26-6
3,3-diethyl-1-(4-iodophenyl)triaz-1-ene

Guidance literature:: p-aminoiodobenzene; With tert.-butylnitrite; boron trifluoride diethyl etherate;

diethylamine; With potassium carbonate;
DOI:10.1081/SCC-200046517

Reference yield:

: 53694-87-4
1-azido-4-iodo-benzene

: 109-89-7
diethylamine

: 630104-26-6
3,3-diethyl-1-(4-iodophenyl)triaz-1-ene

Guidance literature:: With potassium carbonate; In water; acetonitrile; at 0 - 20 ℃; for 2h;
DOI:10.1021/jo4023809

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 630104-26-6
3,3-diethyl-1-(4-iodophenyl)triaz-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0.75 h / 0 °C

2: potassium carbonate / acetonitrile; water / 2 h / 0 - 20 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In water; acetonitrile;
DOI:10.1021/jo4023809