N-(2-(3,4-DIMETHOXYPHENYL)ETHYL)(2-NITROPHENYL)FORMAMIDE

Base Information

• Chemical Name: N-(2-(3,4-DIMETHOXYPHENYL)ETHYL)(2-NITROPHENYL)FORMAMIDE
• CAS No.: 19007-49-9
• Molecular Formula: C17H18N2O5
• Molecular Weight: 330.34
• Mol file: 19007-49-9.mol

Synonyms:2-Nitro-benzoesaeure-<2-(3,4-dimethoxy-phenyl)-aethyl>-amid;N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide;N-(3,4-DIMETHOXYPHENETHYL)-2-NITROBENZENECARBOXAMIDE;2-nitro-benzoic acid-(3,4-dimethoxy-phenethylamide);2-Nitro-benzoesaeure-(3,4-dimethoxy-phenaethylamid);N-[2-(3,4-dimethoxyphenyl)ethyl]-2-nitrobenzamide;2-Nitro-N-(3.4-dimethoxy-phenaethyl)-benzamid;

Chemical Property of N-(2-(3,4-DIMETHOXYPHENYL)ETHYL)(2-NITROPHENYL)FORMAMIDE

Chemical Property:

• PSA: 93.38000
• LogP: 3.49860

Purity/Quality:

99% ^*data from raw suppliers

N-(2-(3,4-dimethoxyphenyl)ethyl)(2-nitrophenyl)formamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2-(3,4-DIMETHOXYPHENYL)ETHYL)(2-NITROPHENYL)FORMAMIDE

There total 8 articles about N-(2-(3,4-DIMETHOXYPHENYL)ETHYL)(2-NITROPHENYL)FORMAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ortho-nitrobenzoic acid (552-16-9,104810-18-6) + 2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) → N-<(3,4-Dimethoxyphenyl)ethyl>-2-nitrobenzamide (19007-49-9)

Guidance literature:

ortho-nitrobenzoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 12h;

2-(3,4-dimethoxyphenyl)-ethylamine; In N,N-dimethyl-formamide; for 12h;

DOI:10.1021/ol053033y

Reference yield:

2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) + 2-nitrobenzyl chloride (610-14-0) → N-<(3,4-Dimethoxyphenyl)ethyl>-2-nitrobenzamide (19007-49-9)

Guidance literature:

Reference yield:

3,4-dimethoxy-benzaldehyde (120-14-9) → N-<(3,4-Dimethoxyphenyl)ethyl>-2-nitrobenzamide (19007-49-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 80 percent / ammonium acetate; acetic acid / 1.5 h / Heating

2.1: LiAlH₄ / tetrahydrofuran / 3 h / Heating

3.1: HOBt; DCC / dimethylformamide / 12 h

3.2: 95 percent / dimethylformamide / 12 h

With ammonium acetate; lithium aluminium tetrahydride; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/ol053033y

upstream raw materials:

2-(3,4-dimethoxyphenyl)-ethylamine

2-nitrobenzyl chloride

ortho-nitrobenzoic acid

3,4-dimethoxynitrostyrene

Downstream raw materials:

6,7-dimethoxy-1-<(ortho-nitro)phenyl>-3,4-dihydroisoquinoline

3-<β-(3,4-Dimethoxyphenyl)ethyl>-3,4-dihydro-4(3H)-oxoquinazoline

N-[2-(6,7-dimethoxy-3,4-dihydroisoquinolin-1-yl)phenyl]hydroxylamine

2-(6,7-dimethoxy-3,4-dihydroisoquinolin-1-yl)phenylamine

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