2-Propanone, 1-(2-cyclohexylideneethoxy)-3-diazo-

Base Information

Chemical Name:2-Propanone, 1-(2-cyclohexylideneethoxy)-3-diazo-
CAS No.:192195-13-4
Molecular Formula:C11H16N2O2
Molecular Weight:208.26
Hs Code.:

Synonyms:

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Chemical Property of 2-Propanone, 1-(2-cyclohexylideneethoxy)-3-diazo-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-Propanone, 1-(2-cyclohexylideneethoxy)-3-diazo-

There total 4 articles about 2-Propanone, 1-(2-cyclohexylideneethoxy)-3-diazo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1552-92-7
ethyl cyclohexylideneacetate

: 192195-13-4
1-(2-cyclohexylideneethoxy)-3-diazo-2-propanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / CH₂Cl₂ / -78 °C

2.1: 89 percent / Rh₂(O₂CCPh₃)4 / CH₂Cl₂ / 0.33 h / 20 °C

3.1: aq. LiOH / methanol / 20 °C

4.1: isobutyl chloroformate; Et₃N / diethyl ether / 3 h / 20 °C

4.2: 434 mg / diethyl ether / 20 °C

With lithium hydroxide; diisobutylaluminium hydride; triethylamine; isobutyl chloroformate; dirhodium(II) tetrakis(triphenylacetate); In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo049900e

Reference yield:

: 932-89-8
2-cyclohexylidene ethanol

: 192195-13-4
1-(2-cyclohexylideneethoxy)-3-diazo-2-propanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / Rh₂(O₂CCPh₃)4 / CH₂Cl₂ / 0.33 h / 20 °C

2.1: aq. LiOH / methanol / 20 °C

3.1: isobutyl chloroformate; Et₃N / diethyl ether / 3 h / 20 °C

3.2: 434 mg / diethyl ether / 20 °C

With lithium hydroxide; triethylamine; isobutyl chloroformate; dirhodium(II) tetrakis(triphenylacetate); In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo049900e

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: (2-cyclohexylidene-ethoxy)-acetic acid

: 192195-13-4
1-(2-cyclohexylideneethoxy)-3-diazo-2-propanone

Guidance literature:: (2-cyclohexylidene-ethoxy)-acetic acid; With triethylamine; isobutyl chloroformate; In diethyl ether; at 20 ℃; for 3h;

diazomethane; In diethyl ether; at 20 ℃;
DOI:10.1021/jo049900e