1-methylpiperazin-2-one trifluoroacetate

Base Information

• Chemical Name: 1-methylpiperazin-2-one trifluoroacetate
• CAS No.: 194350-88-4
• Molecular Formula: C5H10N2O.C2HF3O2
• Molecular Weight: 228.171
• Mol file: 194350-88-4.mol

Synonyms:N-methylpiperazin-2-one trifluoroacetic acid;1-methylpiperazin-2-one trifluoroacetate;4-methyl-3-oxopiperazin-1-ium monotrifluoroacetate;N-methylpiperazin-2-one trifluoroacetic acid salt;

Chemical Property of 1-methylpiperazin-2-one trifluoroacetate

Chemical Property:

• PSA: 69.64000
• LogP: -0.05200

Purity/Quality:

98%min ^*data from raw suppliers

1-Methylpiperazin-2-one trifluoroacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-methylpiperazin-2-one trifluoroacetate

There total 3 articles about 1-methylpiperazin-2-one trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-methylpiperazin-2-one hydrochloride (109384-27-2,1185292-91-4) → 4-methyl-3-oxopiperazin-1-ium monotrifluoroacetate (194350-88-4)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield: 100.0%

1-tert-butoxycarbonyl-4-methyl-3-oxopiperazine (109384-26-1) + trifluoroacetic acid (76-05-1) → 4-methyl-3-oxopiperazin-1-ium monotrifluoroacetate (194350-88-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 1.5h;

Reference yield: 100.0%

→ 4-methyl-3-oxopiperazin-1-ium monotrifluoroacetate (194350-88-4)

Guidance literature:

upstream raw materials:

1-tert-butoxycarbonyl-4-methyl-3-oxopiperazine

trifluoroacetic acid

1-methylpiperazin-2-one hydrochloride

Downstream raw materials:

trans-{4-[4-(4-amino-5-iodo-pyrazolo[2,3-d]pyrimidin-7-yl)-cyclohexyl]}-1-methyl-piperazin-2-one

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