Benzylmesityl ether

Base Information

• Chemical Name: Benzylmesityl ether
• CAS No.: 19578-76-8
• Molecular Formula: C16H18O
• Molecular Weight: 226.318
• Hs Code.: 2909309090
• Mol file: 19578-76-8.mol

Synonyms:2-(Benzyloxy)-1,3,5-trimethylbenzene;Benzene,1,3,5-trimethyl-2-(phenylmethoxy);Benzylmesityl ether;

Chemical Property of Benzylmesityl ether

Chemical Property:

• PSA: 9.23000
• LogP: 4.19080

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzylmesityl ether

There total 5 articles about Benzylmesityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Mesitol (527-60-6) + benzyl bromide (100-39-0) → 2-benzyloxy-1,3,5-trimethylbenzene (19578-76-8) + 2-benzyl-2,4,6-trimethylcyclohexa-3,5-dien-1-one (41388-92-5) + 4-benzyl-2,4,6-trimethylcyclohexa-2,5-dien-1-one (41389-02-0)

Guidance literature:

Mesitol; With n-butyllithium; In hexane; for 0.25h; Inert atmosphere;

benzyl bromide; at 80 ℃; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2021.131935

Reference yield:

Mesitol (527-60-6) + benzyl bromide (100-39-0) → 2-benzyloxy-1,3,5-trimethylbenzene (19578-76-8)

Guidance literature:

Mesitol; With potassium carbonate; In N,N-dimethyl-formamide; for 2h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 60 ℃; for 12h;

DOI:10.1021/jo801659g

Reference yield:

6-acetoxy-2,4,6-trimethyl-cyclohexa-2,4-dienone (4906-82-5) + benzyl chloride (100-44-7) → 2-benzyloxy-1,3,5-trimethylbenzene (19578-76-8)

Guidance literature:

With magnesium; In diethyl ether;

DOI:10.1021/jo00428a030

upstream raw materials:

6-acetoxy-2,4,6-trimethyl-cyclohexa-2,4-dienone

benzyl chloride

Mesitol

benzyl bromide

Downstream raw materials:

3-Benzyl-2.4.6-trimethyl-phenol

mesityl acetate

toluene