CHEMBRDG-BB 5924324

Base Information

• Chemical Name: CHEMBRDG-BB 5924324
• CAS No.: 19615-50-0
• Molecular Formula: C10H12O4
• Molecular Weight: 196.20000
• Hs Code.: 2932190090
• Mol file: 19615-50-0.mol

Synonyms:2-Methyl-3-ethoxycarbonyl-5-acetylfuran;<2-Methyl-3-carbethoxy-<5>furyl>-methyl-keton;5-Acetyl-2-methyl-furan-2-carbonsaeure-ethylester;ETHYL 5-ACETYL-2-METHYL-3-FUROATE;5-acetyl-2-methyl-furan-3-carboxylic acid ethyl ester;

Chemical Property of CHEMBRDG-BB 5924324

Chemical Property:

• Vapor Pressure: 0.000917mmHg at 25°C
• Boiling Point: 303.7oC at 760 mmHg
• Flash Point: 137.5oC
• PSA: 56.51000
• Density: 1.124g/cm3
• LogP: 1.96730

Purity/Quality:

98% ^*data from raw suppliers

ethyl5-acetyl-2-methyl-3-furoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 5924324

There total 10 articles about CHEMBRDG-BB 5924324 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-methyl-3-ethoxycarbonyl-5-ethylidene-4,5-dihydrofuran (122132-65-4) → ethyl 2-methyl-5-acetylfuran-3-carboxylate (19615-50-0) + 5-(1-hydroxyethyl)-3-ethoxycarbonyl-2-methylfuran (130533-22-1) + 5-(1-hydroperoxyethyl)-3-ethoxycarbonyl-2-methylfuran (130533-19-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); oxygen; In benzene; at 50 ℃;

DOI:10.1016/S0040-4020(97)10135-1

Reference yield: 63.0%

ethyl 5-acetyl-2-methyl-4,5-dihydrofuran-3-carboxylate (224424-74-2) → ethyl 2-methyl-5-acetylfuran-3-carboxylate (19615-50-0)

Guidance literature:

With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 - 20 ℃; for 19h;

DOI:10.3987/COM-98-8430

Reference yield: 56.0%

5-(1-hydroperoxyethyl)-3-ethoxycarbonyl-2-methylfuran (130533-19-6) → ethyl 2-methyl-5-acetylfuran-3-carboxylate (19615-50-0)

Guidance literature:

for 20h; Ambient temperature; soybean lipoxygenase, borate buffer, pH=9;

DOI:10.1016/S0040-4039(00)74178-5

upstream raw materials:

5-Eth-(E)-ylidene-2-methyl-4,5-dihydro-furan-3-carboxylic acid ethyl ester

5-(1-hydroperoxyethyl)-3-ethoxycarbonyl-2-methylfuran

2,4-dimethyl-5-acetyloxazole

propynoic acid ethyl ester

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